In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 6575-13-9 as follows. SDS of cas: 6575-13-9
2,6-Dimethylbenzonitrile (10 g, 76.2 mmol),N-Bromosuccinimide (12.074 g, 68.6 mmol) and azobisisobutyronitrile (0.563 g, 3 mmol) were dissolved in anhydrous chloroform (241.42 mL), reacted at 65 C for 4 hours and extracted with dichloromethane After drying with anhydrous magnesium sulfate, purification was carried out by chromatography on silica gel (SiO2, n-Hexane: THF = 9: 1) to remove the side products to obtain a product.
According to the analysis of related databases, 6575-13-9, the application of this compound in the production field has become more and more popular.