Related Products of 6136-93-2,Some common heterocyclic compound, 6136-93-2, name is 2,2-Diethoxyacetonitrile, molecular formula is C6H11NO2, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
To a solution of diethoxyacetonitrile (1 ,120 g, 930 mmol) in MeOH (500 ml_) was added a 17% solution of (NH4)2S in H20 (440 ml_) at rt. The mixture was stirred at rt overnight. The mixture was evaporated in vacuo to approximately 100 ml_ volume and filtered. The solid was washed with cooled water and dried in vacuo to afford the title compound 2 (92 g, 61 %) as a white solid, which was used as such in next step.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 2,2-Diethoxyacetonitrile, its application will become more common.