Reference of 6587-24-2, The chemical industry reduces the impact on the environment during synthesis 6587-24-2, name is Methyl 2-cyanobenzoate, I believe this compound will play a more active role in future production and life.
The mixture of 3.29 gmethyl 2-cyanobenzoate 4 (20.4 mmol), 60 cm3 MeOH,and 22 cm3 1 M NaOH was stirred overnight, and thenconcentrated in vacuo. The residue was diluted with100 cm3 H2O and 100 cm3 DCM, and then acidified with22 cm3 1 M HCl under cooling. The resulting precipitatewas collected, washed with 100 cm3 H2O, 100 cm3 petroleumether and dried to afford 2.60 g (87%)2-cyanobenzoic acid 5 as a white crystalline powder. M.p.:228-230 C ([54] 227-228 C). 1H and 13C NMR spectrawere found to be identical with the ones described in [69].
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Methyl 2-cyanobenzoate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Tkachuk, Volodymyr A.; Hordiyenko, Olga V.; Omelchenko, Irina V.; Medviediev, Volodomir V.; Arrault, Axelle; Monatshefte fur Chemie; vol. 149; 12; (2018); p. 2293 – 2309;,
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