Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3047-38-9, name is Cyclopent-1-enecarbonitrile, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C6H7N
To a stirred solution of cyclopent- l-enecarbonitrile (50 g, 537 mmol) in carbon tetrachloride (400 ml) at 25C was added N-bromosuccinimide (96 g, 537 mmol) under nitrogen atmosphere. The resulting mixture was refluxed for 2 h. The progress of reaction was monitored by TLC. The reaction mixture was cooled to 25C and filtered through Celite. The filtrate was concentrated under reduced pressure to obtain a crude product, which was purified by column chromatography over silica gel ( 100 – 200 mesh) using 1% ethyl acetate in hexane as an eluent to obtain the title compound (60 g, 65%). iHNMR (CDCls, 400MHz): delta 6.77-6.73 (m, IH), 5. 12-5.09 (m, IH) 2.95-2.86 (m, lH) 2.67-2.42 (m, 3H).
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 3047-38-9.
Reference:
Patent; LUPIN LIMITED; JANA, Gourhari; SINHA, Neelima; KARCHE, Navnath, Popat; KURHADE, Sanjay, Pralhad; TILEKAR, Ajay, Ramchandra; GUPTA, Nishant, Ramniwasji; IRLAPATI, Nageswara, Rao; KUKREJA, Gagan; PALLE, Venkata, P.; KAMBOJ, Rajender, Kumar; (102 pag.)WO2016/12956; (2016); A1;,
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