Dulou, Raymond; Savostianoff, Dimitri published the artcile< Synthesis of glyoxal acetals from diethoxyacetonitrile>, Computed Properties of 6136-93-2, the main research area is .
A series of RCOCH(OEt)2 (I) was prepared from (EtO)2CHCN (II) with the corresponding RMgX. II was obtained in 77% yield by ammonolysis of (EtO)2CHCO2Et and subsequent dehydration of the resulting (EtO)2CHCONH2. II (12.9 g.) in 150 cc. dry Et2O added to about 0.2 mol appropriate RMgX in Et2O (1-1.9 mol/kg.), stirred 1 h., kept 12 h. at room temperature, treated with 50 g. NH4Cl in 200 cc. H2O, and acidified with concentrated HCl to pH 2-3 yielded 80-95% corresponding I listed in the table. R, b.p./mm., n20D, d2020, % yield; Et, 98-100°/55, 1.408, 0.929, 80; iso-Pr, 103-4°/45, 1.408, 0.910, 79; Am, 104-7°/9, 1.420, 0.913, 94; C7H15, 126-30°/10-11, 1.426, 0.886, 94; Ph, 135-6°/12, 1.505, 1.040, 80; cyclohexyl, 108-13°/10, 1.448, 0.961, 95;
Comptes Rendus des Seances de l’Academie des Sciences, Serie C: Sciences Chimiques published new progress about 6136-93-2. 6136-93-2 belongs to class nitriles-buliding-blocks, and the molecular formula is C6H11NO2, Computed Properties of 6136-93-2.
Referemce:
Nitrile – Wikipedia,
Nitriles – Chemistry LibreTexts