Scettri, Arrigo published the artcileMukaiyama-Michael vinylogous additions to nitroalkenes under solvent-free conditions, Application In Synthesis of 5153-73-1, the publication is Central European Journal of Chemistry (2012), 10(1), 47-53, database is CAplus.
The first Mukaiyama-Michael vinylogous reaction of a dioxin-derived silyl ether to nitroalkenes is reported. The conjugate addition is performed in absence of a catalyst under solvent-free conditions. Using as starting materials silyl enol ether (i.e., masked acetoacetate ester) 2,2-dimethyl-4-methylene-6-[(trimethylsilyl)oxy]-4H-1,3-dioxin or 2-[(trimethylsilyl)oxy]furan, the synthesis of the target compounds was achieved with satisfactory efficiency with variously substituted (nitro)alkene derivatives Moreover, an organocatalyst for this Mukaiyama-Michael vinylogous reaction of (trimethylsilyloxy)furan to nitroalkenes was developed [i.e., 4-hydroxydinaphtho[2,1-d:1′,2′-f][1,3,2]dioxaphosphepin 4-oxide, BINOL hydrogen phosphate]. The reaction is promoted by Bronsted acids under solvent-free conditions, providing products in moderate to good yield with variously substituted nitroalkenes.
Central European Journal of Chemistry published new progress about 5153-73-1. 5153-73-1 belongs to nitriles-buliding-blocks, auxiliary class Nitrile,Alkenyl,Nitro Compound,Benzene, name is (E)-4-(2-Nitrovinyl)benzonitrile, and the molecular formula is C9H6N2O2, Application In Synthesis of 5153-73-1.
Referemce:
https://en.wikipedia.org/wiki/Nitrile,
Nitriles – Chemistry LibreTexts